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Table of content 2013

Environment
Identification of Volatile Organic Compounds (VOC) by Gas Chromatography coupled to Mass Spectrometry
Development of a method to quantify perfluorinated compounds and oestrogens present in water by SPE-HPLC-MS/MS
Test method validations of assays in closed tubes
Involvement of siderophores in the dissolution of basaltic glasses

Forensic
Development of a method for the determination of cannabinoids in hairs by GC-MS
Validation of analytical method of cyanide compounds in blood by HS-GC-NPD
Validation of an analytical method to measure the refractive index of glass
Analysis of Mycotoxins in Urine by Liquid Chromatography Coupled with a Q ExactiveTM Ultra-high Resolution Mass Spectrometer
Determination and quantification of clonidine, antihypertensive drug in plasma by GC-MS
Estimation of post-mortem interval by LC/HRMS (QTOF) analysis of cuticular lipids in recent and older insect puparia
Analytical approaches of autopsy samples in a case of supposed suicidal death

General
Characterization of stationary phases functionalized by photochemistry

Health and Safety
Optimization of an analysis method for the determination of N-nitrosamines in rubber
Quantification of 4-chloro-3-methylphenol in industrial aqueous effluent by GC-MS
Optimization for the development of methods to quantify a protein in biological environment by LC-MS/MS

Industrial Analysis
On line mercaptans analyzer in kerosene

Instrumentation
Comparison of optical spectrometers in inductively coupled plasma spectrometry

Materials
Influence of thermal conditions on Argon behavior in TiC matrix
Research of chemical additives to prevent wet creep of plasterboards using holographic interferometry
KrF laser beam fluency characterization on PLD ablation target

Pharmaceutical
Optimization of the separation of combretastatin A-4 cis and trans isomers by Ultra High Liquid Chromatography/Mass Spectrometry (uHPLC/MS)
Study of a potential biomarker for Alzheimer’s disease by LC-MS-MS
Antibiotic condensation: Sulfamethoxazole
Development of an assay of peptides on HPLC-MS to quantify and to verify the influence of different antibiotics on these peptides
Synthesis of anticancer agents with Osmium’s complex
Determination of the absolute structure of a compound by single-crystal X-ray diffraction
Qualitative development of Photo-SRM method peptide analysis
Elaboration of an internal quality control for quantification of citric acid in the serum on an automate ABX Pentra 400
Adaptation of the assay of hydroxychloroquine by LC-MS
Comparison of two analyzers for the quantification of anti-HBs antibodies using ELISA method
Optimization of enzymatic digestion by LC-MS-MS

Quality
Quantification of Stepantex of 1H NMR spectroscopy
Internal control making for the search of Brucellosis into cow milk by ELISA method
Validation of Doxorubicin’s calibration ranges using the automatic diluter in Spectroscopy UV-Raman for pre-release dosage formulations of anticancer drugs
Quantification of alkylphenols ethoxylate in textiles by HPLC/MS/MS
Validation of an HPLC method to quantify D-penicillamine
Validation of UV spectroscopic method for estimation of azithromycin
Glass pearl analysis by means of LIBS technology
Analysis of soap weight loss with water-content measures by Karl Fisher titrator as part of quality control

Sustainable Development
Use of green solvent in Arizona systems for Countercurrent Chromatography
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Special Highlight


Estimation of post-mortem interval by LC/HRMS (QTOF) analysis of cuticular lipids in recent and older insect puparia
The purpose of this study is to investigate if an alteration of empty pupae lipidic content occurring with time can be observed. There is also a possible application to estimate the post-mortem interval (PMI).
Preliminary studies conducted by GC/MS have shown that the decomposition of the pupa...

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Characterization of stationary phases functionalized by photochemistry
Monoliths are used as a new stationary phase which enable the miniaturization of systems and give good performances. The advantage of that kind of stationary phase is that their synthesis can be done in-situ, thus, the silanisation is directly created into a 75 micron capillary. ...

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Quantification of 4-chloro-3-methylphenol in industrial aqueous effluent by GC-MS
As endocrine disruptors, chlorophenols can endanger water environments. This is why these pollutants are subject to rigorous controls, especially for industrial wastewaters.
However, it is not advised to analyze them by GC without preparation because of their high polarity which produces a bro...

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Development of an assay of peptides on HPLC-MS to quantify and to verify the influence of different antibiotics on these peptides
Staphylococcus aureus is a bacterium responsible for many types of infections, such as nosocomial infections in humans. Plus, it is the second pathogen responsible for this type of infection after Escherichia coli. S. aureus has the ability to secrete, after invasion, adhesion factors, toxins or enz...

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