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Table of content 2011

Biology
Enaminone analysis by 1H NMR spectroscopy
Determination of cocaine in several matrices
Qualification of a thin layer chromatography system using a radioactivity detector
Validation of an analytical method for the titration of anti retroviral drug
Optimization of a dynamic coupling of ATIII and improvement of the efficiency of an affinity column
The feasibility of the nucleosides assay in PBMCs by analysing with LC-MS/MS
Quantifying aromatic amines in the follow-up of professional expositions
Quantifying ethanol by HS-GC-FID in peripheral blood of victim
Developing a sample preparation method in SPE to quantify a protein in human urine by LC-MS/MS
Precision of the Methotrexate measurement
Comparison of two spectrophotometers with DNA concentration measures from total blood
Verification on site of a HPLC robot for the assay of glycosylated hemoglobin.

Environment
Titration of total hydrocarbons (C10 to C40) using GC-FID
Developing a conductometric biosensor to analyze formaldehyde in an aquatic environment
Extraction and quantification of Polycyclic Aromatic Hydrocarbons in HPLC
Development of a new passive sampler for pesticides quantification in water samples
Detection of PCB (polychlorinated biphenyl)

Food
Determine protein content in high protein creams by the Kjeldahl method
A rapid analytical method to study the chelation of calcium by complexing agents like emulsifying salts
Search for and quantification of microorganisms in processed food
Analysis of green immature soybeans for their content in sucrose and glutamate

Forensic
Research of organic explosives, by HPTLC, on white cloth soiled with blood
Identification and comparison of several gasoline samples by GC-FID
Highlighting and identifying petroleum distillates into fire-charred residues

Pharmaceutical
Adapting extraction SPE and GC-MS analysis methods to search Promethazine in hair
Developing a High Performance Liquid Chromatography method to quantify Vancomycin
Optimising and validating a method for the HPLC assay of an active molecule in order to achieve its forced degradation
Transfer of an analytical method to the workshop
Extraction and analysis of an antileish-maniasis natural substance from a Guyanese plant in NMR

Quality
Validation of analytical methods of a chemistry automated in a medical analysis laboratory
Determination of a laboratory internal repeatability and comparison with standards

Sustainable development
Analysis of Somalia Incense essential oil by gas chromatography and physicochemical measurements
Capture and storage of carbon dioxide in minerals

Sustainable Development
Method optimasation and sugar analyses by liquid chromatography with refractive index detection

Toxicology
Cannabis assay in biological samples by GC/MS
MANCO



Special Highlight


Quantifying aromatic amines in the follow-up of professional expositions
Aromatic amines had been used for a long time in several fields. O-toluidine and aniline are above all used in pharmaceutical and phytosanitary industries to produce drugs or colouring agents. The three other studied compounds, 2,4- and 2,6-TDA and MDA are used in polyurethane synthesis.
Althou...

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Developing a sample preparation method in SPE to quantify a protein in human urine by LC-MS/MS
One of the themes of the research in mass spectrometry of the team « Anabio » in the “Laboratoire des Sciences Analytiques”, is to develop and validate methods to measure biomarkers in human complex matrixes (blood, urine, plasma, serum…). Urine has become one of the most attractive biofluids as it ...

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A rapid analytical method to study the chelation of calcium by complexing agents like emulsifying salts
Processed cheese spread is a common product in the world, and its sales have been growing for over a century. It is a product of second transformation and is also longlife. Its nutritional value and taste make this cheese very pleasant, more particularly to children. However, the role of all the ing...

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Extraction and analysis of an antileish-maniasis natural substance from a Guyanese plant in NMR
Leishmaniasis is a skin disease, which is caused by an intracellular parasite, leishmania. It is generally transmitted by the bite of a female of the phlebotominae family. Irlbachia alata (I.alata) is an ubiquitous herb found in Central and Tropical South America. The plant is commonly used by indig...

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